Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 291 |
| Detector technology | PIXEL |
| Collection date | 2023-05-20 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97853 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 66.816, 66.816, 375.520 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 55.300 - 2.638 |
| R-factor | 0.2269 |
| Rwork | 0.221 |
| R-free | 0.27940 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.405 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.16_3549: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 57.190 | 2.780 |
| High resolution limit [Å] | 2.638 | 2.640 |
| Rmerge | 0.200 | 1.800 |
| Rmeas | 0.209 | 1.864 |
| Rpim | 0.036 | 0.372 |
| Number of reflections | 15861 | 2239 |
| <I/σ(I)> | 17.7 | 2.3 |
| Completeness [%] | 100.0 | |
| Redundancy | 31.9 | |
| CC(1/2) | 0.999 | 0.812 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 1.6 M Potassium/Sodium phosphate pH 6.5 |
