8YYO

Crystal structure of TsaGH11 complexed with beta-D-xylopyranose (Data II)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2019-04-04
Detector	ADSC QUANTUM 270
Wavelength(s)	0.9793
Spacegroup name	P 43 21 2
Unit cell lengths	73.226, 73.226, 164.778
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.400 - 1.700
R-factor	0.1663
Rwork	0.165
R-free	0.19360
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.853
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.730
High resolution limit [Å]	1.700	1.700
Number of reflections	49993	2406
<I/σ(I)>	9.98
Completeness [%]	99.7
Redundancy	18.7
CC(1/2)	0.996	0.623

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		295	ammonium acetate, Tris-HCl