8YT5
SP1746 treated with EDTA, in complex with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-01-28 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 0.984050 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 69.271, 69.271, 88.463 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.010 - 1.600 |
R-factor | 0.19407 |
Rwork | 0.194 |
R-free | 0.20216 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.230 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.010 | 1.640 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 32997 | 2407 |
<I/σ(I)> | 31.97 | |
Completeness [%] | 100.0 | |
Redundancy | 19.1 | |
CC(1/2) | 0.999 | 0.843 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 287.2 | 20% PEG3350,0.2 M Potassium sulfate |