8YQJ

Crystal structure of HylD1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL02U1
Synchrotron site	SSRF
Beamline	BL02U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-01-13
Detector	DECTRIS EIGER2 S 9M
Wavelength(s)	0.9791
Spacegroup name	P 21 21 21
Unit cell lengths	57.299, 68.751, 124.387
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	35.510 - 1.690
R-factor	0.1984
Rwork	0.197
R-free	0.23480
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.011
Data reduction software	xia2
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	35.940	1.730
High resolution limit [Å]	1.690	1.690
Number of reflections	52594	2658
<I/σ(I)>	9.3
Completeness [%]	94.4
Redundancy	9.5
CC(1/2)	0.989	0.368

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		292	Tacsimate, MES monohydrate, PEG 4000