8YQE

CDK2 and small molecular inhibitor L56

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-07-10
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9785
Spacegroup name	P 21 21 21
Unit cell lengths	53.754, 72.042, 72.737
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.230 - 1.940
R-factor	0.2019
Rwork	0.200
R-free	0.24170
Structure solution method	SIRAS
RMSD bond angle	10.332
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.230	1.990
High resolution limit [Å]	1.940	1.940
Rmerge	0.063	0.284
Number of reflections	21552	1423
<I/σ(I)>	27.1
Completeness [%]	99.9
Redundancy	12.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		289	PEG3350,Hepes 7.4