8YQC

Galectin-10 C29AC57A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-06-30
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97853
Spacegroup name	P 65 2 2
Unit cell lengths	48.824, 48.824, 261.403
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.600 - 1.920
R-factor	0.2071
Rwork	0.204
R-free	0.23810
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.257
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.600	1.970
High resolution limit [Å]	1.920	1.920
Rmerge	0.106	0.778
Number of reflections	14988	995
<I/σ(I)>	18.4
Completeness [%]	98.2
Redundancy	16.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG