8YQB

Galectin-10 N32A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-06-30
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97853
Spacegroup name	P 65 2 2
Unit cell lengths	48.981, 48.981, 263.283
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.670 - 1.950
R-factor	0.1942
Rwork	0.192
R-free	0.21870
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.179
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.670	2.000
High resolution limit [Å]	1.950	1.950
Rmerge	0.142	0.600
Number of reflections	14787	987
<I/σ(I)>	13.2
Completeness [%]	99.9
Redundancy	13.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG