8YQA

Galectin-10 L27A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-06-30
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97853
Spacegroup name	P 65 2 2
Unit cell lengths	48.679, 48.679, 259.791
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.530 - 2.170
R-factor	0.2101
Rwork	0.206
R-free	0.24920
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.081
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.980	2.240
High resolution limit [Å]	2.170	2.170
Rmerge	0.187	0.705
Number of reflections	10513	895
<I/σ(I)>	16.3
Completeness [%]	98.7
Redundancy	30.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG