Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-05-24 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 1 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 53.481, 70.006, 71.898 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.980 - 1.800 |
| R-factor | 0.1837 |
| Rwork | 0.182 |
| R-free | 0.22030 |
| Structure solution method | SIRAS |
| RMSD bond angle | 14.114 |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.950 | 1.830 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.020 | 0.060 |
| Number of reflections | 25752 | 1426 |
| <I/σ(I)> | 22.8 | |
| Completeness [%] | 99.7 | |
| Redundancy | 1.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 289 | PEG3350,Hepes 7.4 |
