8YO0
Crystal Structure of Human Rab23 Y79del in Complex with GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-X |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-01-19 |
Detector | RIGAKU HyPix-6000HE |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.787, 51.606, 74.597 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.640 - 1.300 |
R-factor | 0.1595 |
Rwork | 0.158 |
R-free | 0.18580 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.126 |
Data reduction software | CrysalisPro |
Data scaling software | CrysalisPro |
Phasing software | PHASER |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.640 | 1.320 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.086 | 1.025 |
Rmeas | 0.094 | 1.153 |
Rpim | 0.038 | 0.519 |
Total number of observations | 225700 | 9419 |
Number of reflections | 39490 | 1954 |
<I/σ(I)> | 11.2 | 1.9 |
Completeness [%] | 99.9 | |
Redundancy | 5.7 | 4.8 |
CC(1/2) | 0.999 | 0.593 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 0.1M SPG pH 5.0, 27.5% PEG 1500 |