8YNG

CDK2 and compounds and inhibors

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-10-21
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9792
Spacegroup name	P 21 21 21
Unit cell lengths	53.550, 71.280, 71.770
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	35.640 - 1.820
R-factor	0.1938
Rwork	0.190
R-free	0.23540
Structure solution method	SIRAS
RMSD bond length	0.008
RMSD bond angle	1.028
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	35.640	1.870
High resolution limit [Å]	1.820	1.820
Rmerge	0.126	1.157
Number of reflections	25313	1842
<I/σ(I)>	13.8
Completeness [%]	100.0
Redundancy	11.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	PEG3350,Hepes 7.4