8YMD

Galectin-3 with lychnose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-10-31
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9793
Spacegroup name	P 21 21 21
Unit cell lengths	35.886, 57.383, 61.716
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	17.130 - 1.080
R-factor	0.1415
Rwork	0.141
R-free	0.15890
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.150
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.020	1.100
High resolution limit [Å]	1.080	1.080
Rmerge	0.049	0.206
Number of reflections	55329	2719
<I/σ(I)>	45.7
Completeness [%]	100.0
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG