Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL02U1 |
| Synchrotron site | SSRF |
| Beamline | BL02U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-01-09 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.987 |
| Spacegroup name | P 1 |
| Unit cell lengths | 38.347, 92.608, 95.219 |
| Unit cell angles | 75.02, 89.28, 79.82 |
Refinement procedure
| Resolution | 91.930 - 2.090 |
| R-factor | 0.26507 |
| Rwork | 0.262 |
| R-free | 0.32452 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.724 |
| Data reduction software | HKL-3000 (7.21) |
| Data scaling software | HKL-3000 (7.21) |
| Phasing software | PHASER (2.7.0) |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 91.930 | 2.118 |
| High resolution limit [Å] | 2.090 | 2.090 |
| Rmerge | 0.051 | 0.030 |
| Number of reflections | 68329 | 2644 |
| <I/σ(I)> | 14.3 | |
| Completeness [%] | 97.5 | |
| Redundancy | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 293 | PEG3350, 50 mM potassium phosphate (pH 7.5), 5% glycerol, 4% DMSO |
