8YFK
Crystal structure of FIP200 claw/TNIP1_FIR_pS123
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-05-19 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 |
Unit cell lengths | 37.812, 45.936, 72.951 |
Unit cell angles | 81.20, 89.67, 88.74 |
Refinement procedure
Resolution | 37.800 - 2.000 |
R-factor | 0.1845 |
Rwork | 0.183 |
R-free | 0.21960 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.843 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.16_3549: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.800 | 2.071 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.042 | 0.298 |
Rmeas | 0.064 | |
Number of reflections | 31812 | 3108 |
<I/σ(I)> | 14 | 2.9 |
Completeness [%] | 97.2 | 95.8 |
Redundancy | 3.4 | 2.1 |
CC(1/2) | 0.994 | 0.908 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.018M magnesium chloride hexahydrate, 0.018M calcium chloride dehydrate, 0.1M imidazole, 0.1M MES, 0.1M monohydrate, 10% v/v MPD, 10% PEG 1000, 10% v/v PEG 3350, pH 6.5 |