8YEW
TRIP4 ASCH domain in unliganded form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL02U1 |
Synchrotron site | SSRF |
Beamline | BL02U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-04-17 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 29.387, 67.487, 73.012 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.630 - 1.900 |
R-factor | 0.2091 |
Rwork | 0.207 |
R-free | 0.25390 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.901 |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.560 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.123 | 0.546 |
Rmeas | 0.147 | 0.649 |
Rpim | 0.079 | 0.344 |
Total number of observations | 33045 | 4942 |
Number of reflections | 11259 | 1656 |
<I/σ(I)> | 5.7 | 2.6 |
Completeness [%] | 94.9 | |
Redundancy | 2.9 | 3 |
CC(1/2) | 0.992 | 0.735 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | 0.2 M Li2SO4, 0.1 M Tris HCl (pH 8.5), and 30% (w/v) polyethylene glycol (PEG) 4,000. |