8YA8

The crystal structure of human Rtel1 HHD2 domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 11C
Synchrotron site	PAL/PLS
Beamline	11C
Temperature [K]	100
Detector technology	CCD
Collection date	2023-04-04
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	P 1 21 1
Unit cell lengths	66.052, 61.958, 79.953
Unit cell angles	90.00, 95.14, 90.00

Refinement procedure

Resolution	48.900 - 2.850
R-factor	0.2406
Rwork	0.239
R-free	0.26840
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.883
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.17.1_3660: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.950
High resolution limit [Å]	2.850	2.850
Number of reflections	14421	1393
<I/σ(I)>	8.09	1.59
Completeness [%]	94.3
Redundancy	3.8
CC(1/2)	0.999	0.766

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	296.15	0.2 M Potassium sulfate, 20% (v/v) PEG 3350