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8XUL

Structure of beta-1,2-glucanase from Xanthomonas campestris pv. campestris (beta-1,2-glucoheptasaccharide complex)-E239Q mutant

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]100
Detector technologyPIXEL
Collection date2022-02-05
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.0
Spacegroup nameP 43 3 2
Unit cell lengths220.178, 220.178, 220.178
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution49.233 - 2.500
Rwork0.338
R-free0.36460
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.059
RMSD bond angle2.011
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0425)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]49.2332.510
High resolution limit [Å]2.4502.450
Rmerge0.1211.050
Rpim0.0270.233
Number of reflections672084460
<I/σ(I)>33.75
Completeness [%]100.0
Redundancy39.1
CC(1/2)1.0000.949
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP293NaNO3, PEG 3350, Bis-tris propane

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