8XIF
The crystal structure of the AEP domain of VACV D5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL10U2 |
Synchrotron site | SSRF |
Beamline | BL10U2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-05-18 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.987 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.470, 56.620, 74.160 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.310 - 1.390 |
R-factor | 0.18 |
Rwork | 0.179 |
R-free | 0.19720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.048 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.1_4122: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.310 | 1.420 |
High resolution limit [Å] | 1.390 | 1.390 |
Rmerge | 0.098 | 0.098 |
Rmeas | 0.102 | |
Rpim | 0.029 | |
Number of reflections | 45138 | 45138 |
<I/σ(I)> | 13.8 | |
Completeness [%] | 100.0 | |
Redundancy | 12.8 | 13 |
CC(1/2) | 0.998 | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 290 | 0.1 M Magnesium formate dihydrate, 15% w/v Polyethylene glycol 3,350 |