8XIA

X-RAY ANALYSIS OF D-XYLOSE ISOMERASE AT 1.9 ANGSTROMS: NATIVE ENZYME IN COMPLEX WITH SUBSTRATE AND WITH A MECHANISM-DESIGNED INACTIVATOR

Experimental procedure

Spacegroup name	I 2 2 2
Unit cell lengths	94.200, 100.200, 103.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 1.900
R-factor	0.14
RMSD bond length	0.022
RMSD bond angle	0.044
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.141 *
Number of reflections	38364 *
Completeness [%]	98.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	d-xylose isomerase	25 (mg/ml)
2	1	reservoir		0.76 (M)
3	1	reservoir	PIPES	0.01 (M)