8XF3
Crystal structure of the reassembled C-phycocyanin octamer from Thermoleptolyngbya sp. O-77
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL45XU |
Synchrotron site | SPring-8 |
Beamline | BL45XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-04 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | I 4 3 2 |
Unit cell lengths | 230.800, 230.800, 230.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.110 - 2.500 |
R-factor | 0.2038 |
Rwork | 0.202 |
R-free | 0.23960 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 1.145 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 36274 | 5721 |
<I/σ(I)> | 14.3 | |
Completeness [%] | 100.0 | |
Redundancy | 63 | |
CC(1/2) | 0.998 | 0.554 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.6M sodium chloride, 8% polyethylene glycol 6000, 20% glycerol |