8X8V
Crystal structure of Cypovirus Polyhedra mutant fused with c-Myc fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-11-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | I 2 3 |
Unit cell lengths | 106.590, 106.590, 106.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.690 - 2.000 |
R-factor | 0.204 |
Rwork | 0.199 |
R-free | 0.25050 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.824 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 13787 | 1365 |
<I/σ(I)> | 26.1 | |
Completeness [%] | 99.9 | |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.746 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 293 | cell-free crystallization |