8X7S

Crystal structure of tlr0611

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-07-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97915
Spacegroup name	P 41 21 2
Unit cell lengths	99.304, 99.304, 310.684
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.860 - 3.350
R-factor	0.2559
Rwork	0.254
R-free	0.27530
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.677
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.860	3.620
High resolution limit [Å]	3.350	3.350
Rmerge	0.090	0.964
Number of reflections	23126	4680
<I/σ(I)>	11.9
Completeness [%]	99.3
Redundancy	5.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG