Experimental procedure
| Experimental method | LAUE |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL12-2 |
| Synchrotron site | SSRL |
| Beamline | BL12-2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-11-10 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.73 - 1.85 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 356.980, 70.400, 75.810 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 24.880 - 2.800 |
| R-factor | 0.23921 |
| Rwork | 0.236 |
| R-free | 0.28010 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.304 |
| Data reduction software | XDS |
| Data scaling software | Aimless (0.5.31) |
| Phasing software | PHENIX |
| Refinement software | REFMAC (v5.5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.880 | 2.750 |
| High resolution limit [Å] | 2.690 | 2.690 |
| Number of reflections | 53788 | 7963 |
| <I/σ(I)> | 7.49 | 0.59 |
| Completeness [%] | 98.0 | 92.2 |
| Redundancy | 13.16 | 11.77 |
| CC(1/2) | 0.990 | 0.270 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298.15 | pH 4.5, 100mM Na-acetate/acetic acid, 200mM lithium sulfate, 50% (v/v) PEG 400, 0.5uL of 100% PEG 400 |
