8WU6
Structure of a Nerylneryl Diphosphate Synthase from Solanum lycopersicum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL02U1 |
Synchrotron site | SSRF |
Beamline | BL02U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-06-17 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 0.97880 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.370, 125.370, 52.990 |
Unit cell angles | 90.00, 110.09, 90.00 |
Refinement procedure
Resolution | 28.160 - 1.810 |
R-factor | 0.1772 |
Rwork | 0.176 |
R-free | 0.20580 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.959 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1-4487)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 62.680 | 1.910 |
High resolution limit [Å] | 1.810 | 1.810 |
Rmerge | 0.071 | 0.162 |
Number of reflections | 46804 | 6864 |
<I/σ(I)> | 15.8 | 8.1 |
Completeness [%] | 99.2 | |
Redundancy | 6.5 | |
CC(1/2) | 0.997 | 0.980 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.6 | 289.15 | 0.1M BICINE (pH 7.6), 30% v/v PEG monomethyl ether 550, 0.1 M Sodium chloride |