8WPV
Truncated mutant (1-171) of ferritin from Ureaplasma diversum soaked in Fe2+ solution for 30min
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL02U1 |
Synchrotron site | SSRF |
Beamline | BL02U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-10-06 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 0.9791 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 180.599, 180.599, 180.599 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.926 - 2.059 |
R-factor | 0.2199 |
Rwork | 0.217 |
R-free | 0.24910 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.629 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 104.270 | 2.170 |
High resolution limit [Å] | 2.059 | 2.060 |
Rmerge | 0.278 | |
Rmeas | 0.282 | |
Rpim | 0.045 | 0.998 |
Total number of observations | 87898 | |
Number of reflections | 29497 | 2301 |
<I/σ(I)> | 16.3 | 0.9 |
Completeness [%] | 100.0 | |
Redundancy | 38.6 | 38.2 |
CC(1/2) | 0.999 | 0.482 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 279 | Bicine, MgCl2 |