8WA9
Human transketolase soaked with donor ketose D-fructose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-04-06 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.400, 86.400, 92.500 |
Unit cell angles | 90.00, 94.00, 90.00 |
Refinement procedure
Resolution | 24.430 - 1.500 |
R-factor | 0.1629 |
Rwork | 0.162 |
R-free | 0.18730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.061 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.600 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 342211 | 59465 |
<I/σ(I)> | 5.29 | |
Completeness [%] | 94.2 | |
Redundancy | 1.7 | |
CC(1/2) | 0.992 | 0.615 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.9 | 277 | 13.5-15% PEG 6000 (w/v), 4% PEG 400 (v/v), 2 % glycerol (v/v) |