8W6S
Ferritin from Ureaplasma diversum soaking in Fe2+ solution for 2 min
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-05-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.55 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 179.765, 179.765, 179.765 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.941 - 2.099 |
R-factor | 0.1812 |
Rwork | 0.178 |
R-free | 0.21060 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.833 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 10.000 | 2.140 |
High resolution limit [Å] | 2.099 | 5.700 | 2.100 |
Rmerge | 0.200 | 0.101 | 1.800 |
Rmeas | 0.242 | 0.102 | 0.990 |
Rpim | 0.029 | 0.013 | 0.295 |
Number of reflections | 27465 | 886 | 734 |
<I/σ(I)> | 3 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 20 | 15 | 15 |
CC(1/2) | 0.988 | 0.994 | 0.759 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 297 | Bicine, MgCl2 |