8W6B
crystal structure of TAX1BP1 SKICH domain in complex with RB1CC1 coiled-coil domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-16 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97890 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.239, 86.815, 147.860 |
Unit cell angles | 90.00, 95.74, 90.00 |
Refinement procedure
Resolution | 42.700 - 2.390 |
R-factor | 0.1952 |
Rwork | 0.193 |
R-free | 0.23420 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 0.995 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.360 | 2.520 |
High resolution limit [Å] | 2.390 | 2.390 |
Number of reflections | 39479 | 5914 |
<I/σ(I)> | 13.8 | |
Completeness [%] | 97.7 | |
Redundancy | 6.7 | |
CC(1/2) | 0.998 | 0.767 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 5% (w/v) PEG 4000, 50 mM Magnesium chloride, 100 mM MES at pH 6.5, 10% 2-propanol |