Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 173 |
| Detector technology | PIXEL |
| Collection date | 2023-05-03 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 142.720, 139.260, 88.040 |
| Unit cell angles | 90.00, 124.84, 90.00 |
Refinement procedure
| Resolution | 47.090 - 1.976 |
| R-factor | 0.1932 |
| Rwork | 0.192 |
| R-free | 0.21260 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.950 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | BUSTER |
| Refinement software | BUSTER (2.11.8 (22-FEB-2023)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.090 | 2.010 |
| High resolution limit [Å] | 1.976 | 1.976 |
| Number of reflections | 93889 | 3963 |
| <I/σ(I)> | 15 | |
| Completeness [%] | 95.8 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.999 | 0.508 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | ammonium citrate tribasic |
