Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 2 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2023-11-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.729317 |
| Spacegroup name | P 1 |
| Unit cell lengths | 22.434, 22.492, 31.230 |
| Unit cell angles | 104.44, 90.22, 104.74 |
Refinement procedure
| Resolution | 21.010 - 1.210 |
| R-factor | 0.2064 |
| Rwork | 0.201 |
| R-free | 0.24700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.725 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 21.010 | 1.253 |
| High resolution limit [Å] | 1.210 | 1.210 |
| Number of reflections | 16793 | 1682 |
| <I/σ(I)> | 5.63 | |
| Completeness [%] | 96.3 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.996 | 0.474 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | SLOW COOLING | 298 | methanol and water |
