8VFJ
Polymerase Beta Host Guest Complex Containing FapydG base paired with TMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-08-16 |
Detector | DECTRIS PILATUS3 R 200K-A |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.378, 80.890, 58.302 |
Unit cell angles | 90.00, 110.15, 90.00 |
Refinement procedure
Resolution | 24.750 - 2.140 |
R-factor | 0.2151 |
Rwork | 0.211 |
R-free | 0.26490 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.150 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.190 |
High resolution limit [Å] | 2.140 | 2.140 |
Number of reflections | 34645 | 1266 |
<I/σ(I)> | 18.2 | |
Completeness [%] | 98.5 | |
Redundancy | 3.3 | |
CC(1/2) | 0.998 | 0.690 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 14-22% PEG 3350 0.05 M Imidazole pH 8.0 0.35 M Sodium Acetate |