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8VCM

Crystal structure of rMcL-1 in complex with galactose

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]101
Detector technologyPIXEL
Collection date2019-09-27
DetectorDECTRIS PILATUS 200K
Wavelength(s)1.54
Spacegroup nameP 1 21 1
Unit cell lengths57.217, 41.094, 67.938
Unit cell angles90.00, 107.70, 90.00
Refinement procedure
Resolution34.690 - 2.210
R-factor0.1848
Rwork0.184
R-free0.20360
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle1.154
Data reduction softwareHKL-3000
Data scaling softwareHKL-3000
Phasing softwareHKL-3000
Refinement softwarePHENIX (1.21rc1_5156)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.280
High resolution limit [Å]2.2002.200
Rmerge0.119
Number of reflections276972235
<I/σ(I)>27.2
Completeness [%]99.5
Redundancy5
CC(1/2)0.8610.861
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.5291.150.2 M Na iodine, 0.1 M Bis-tris pronane pH 8.5, 20% PEG 3350

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