8V7I
Human DNA polymerase eta-DNA-araC-ended primer ternary complex:reaction with 1 mM Mg2+ for 1800s
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2022-09-21 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 0.9786 |
Spacegroup name | P 61 |
Unit cell lengths | 98.547, 98.547, 81.894 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.670 - 1.720 |
R-factor | 0.2134 |
Rwork | 0.212 |
R-free | 0.23280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.175 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.672 | 42.672 | 1.820 |
High resolution limit [Å] | 1.720 | 5.110 | 1.720 |
Rmerge | 0.056 | 0.022 | 0.714 |
Rmeas | 0.061 | 0.024 | 0.783 |
Number of reflections | 47892 | 3567 | 15111 |
<I/σ(I)> | 20.46 | ||
Completeness [%] | 98.8 | ||
Redundancy | 11.5 | ||
CC(1/2) | 0.999 | 0.999 | 0.773 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | PEG 2000MME, 0.1 M MES |