8V56
UIC-1 mutant - UIC-1-B5W
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-03-12 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.6199 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 16.543, 20.422, 56.557 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.560 - 0.980 |
R-factor | 0.1322 |
Rwork | 0.131 |
R-free | 0.14730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.737 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 16.560 | 1.015 |
High resolution limit [Å] | 0.980 | 0.980 |
Rmerge | 0.083 | 0.863 |
Rmeas | 0.087 | 0.956 |
Rpim | 0.025 | 0.401 |
Number of reflections | 11436 | 1015 |
<I/σ(I)> | 17.5 | 1.43 |
Completeness [%] | 98.5 | |
Redundancy | 11.4 | |
CC(1/2) | 1.000 | 0.598 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SLOW COOLING | 298 | water, acetonitrile |