8UWA
VH1-18 QxxV class antibody 09-1B12 bound to A/Perth/16/2009 H3N2 hemagglutinin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-14 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 158.040, 158.040, 417.206 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.210 - 4.020 |
R-factor | 0.2307 |
Rwork | 0.230 |
R-free | 0.25440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB entries 5KVN & 5K9Q |
RMSD bond length | 0.005 |
RMSD bond angle | 0.721 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.210 | 4.164 |
High resolution limit [Å] | 4.020 | 4.021 |
Number of reflections | 51070 | 4940 |
<I/σ(I)> | 7 | |
Completeness [%] | 99.7 | |
Redundancy | 20.5 | |
CC(1/2) | 0.995 | 0.654 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 15% v/v 2-propanol, 0.1 M sodium citrate tribasic dihydrate, pH 5.0, 10% w/v PEG10000 |