8US1
P21 Crystal structure of TamA from Pseudomonas aeruginosa at 2.6 Ang
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2013-11-07 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97910 Ang |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 78.710, 63.843, 84.010 |
Unit cell angles | 90.00, 108.55, 90.00 |
Refinement procedure
Resolution | 40.900 - 2.650 |
Rwork | 0.200 |
R-free | 0.26000 |
Structure solution method | SAD |
Data reduction software | autoXDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.700 |
High resolution limit [Å] | 2.650 | 7.190 | 2.650 |
Rmerge | 0.115 | 0.046 | |
Number of reflections | 41274 | 1537 | 2793 |
<I/σ(I)> | 12.6 | ||
Completeness [%] | 93.2 | 99.4 | 83.4 |
Redundancy | 4.1 | 5.8 | 2.8 |
CC(1/2) | 0.900 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 293 | 12% peg 4K, 50 mM MgCl2, 70 mM Hepes pH 7.2, 4% isopropanol, 10% glycerol |