8UJW

Crystal structure of the KETc7 antigen from Taenia solium

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-01-27
Detector	DECTRIS EIGER2 X CdTe 16M
Wavelength(s)	1.1950
Spacegroup name	C 1 2 1
Unit cell lengths	124.134, 36.613, 41.472
Unit cell angles	90.00, 103.27, 90.00

Refinement procedure

Resolution	37.810 - 1.720
R-factor	0.201
Rwork	0.198
R-free	0.22880
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.190
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHENIX
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	37.810	1.785
High resolution limit [Å]	1.720	1.724
Rmerge	0.014	0.180
Rmeas	0.020
Rpim	0.014
Number of reflections	18620	1357
<I/σ(I)>	23.39
Completeness [%]	95.9
Redundancy	13.72
CC(1/2)	1.000	0.927

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	0.2 M ammonium acetate, 0.1 M BIS-TRIS 6.5, 25 % w/v PEF 3350