8UHL
ATAD2B bromodomain in complex with histone H4 acetylated at lysine 12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2020-07-19 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 55.119, 55.119, 140.657 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.560 - 1.920 |
Rwork | 0.200 |
R-free | 0.22330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.560 | 1.989 |
High resolution limit [Å] | 1.920 | 1.920 |
Rmerge | 0.109 | |
Rmeas | 0.114 | |
Rpim | 0.031 | |
Number of reflections | 17341 | 1672 |
<I/σ(I)> | 20.22 | |
Completeness [%] | 99.7 | |
Redundancy | 13 | |
CC(1/2) | 0.999 | 0.448 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 1.8 M Ammonium citrate tribasic pH 7 |