8TYH
Plasmodium vivax PMX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-10-30 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9537 |
| Spacegroup name | P 63 |
| Unit cell lengths | 136.299, 136.299, 45.946 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 42.820 - 1.830 |
| R-factor | 0.2292 |
| Rwork | 0.228 |
| R-free | 0.25090 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.019 |
| RMSD bond angle | 0.864 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.610 | 1.870 |
| High resolution limit [Å] | 1.830 | 1.830 |
| Rmerge | 1.485 | |
| Rpim | 0.471 | |
| Number of reflections | 43343 | 2639 |
| <I/σ(I)> | 16.1 | 1.8 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 10.3 | |
| CC(1/2) | 0.999 | 0.712 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4 | 293 | 0.1M SPG 25% (w/v) PEG 1500 30% (v/v) (+/-)-2-Methyl-2,4-pentanediol 1mM TEW |
