Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-04-26 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.95370 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 60.720, 81.850, 192.876 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.770 - 2.590 |
| R-factor | 0.1869 |
| Rwork | 0.184 |
| R-free | 0.24090 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.548 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.770 | 2.687 |
| High resolution limit [Å] | 2.590 | 2.590 |
| Rmeas | 0.139 | |
| Rpim | 0.422 | |
| Number of reflections | 15265 | 1462 |
| <I/σ(I)> | 12.17 | 1.54 |
| Completeness [%] | 99.6 | 97.99 |
| Redundancy | 8 | |
| CC(1/2) | 0.707 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.88 | 293 | 20% PEG 3350 0.2M Na2HPO4/KH2PO4 |
