8TXM
Crystal structure of 05.GC.w13.02 Fab in complex with H1 HA from A/California/04/2009(H1N1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-23 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97934 |
Spacegroup name | P 21 3 |
Unit cell lengths | 167.531, 167.531, 167.531 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.770 - 3.250 |
R-factor | 0.2759 |
Rwork | 0.275 |
R-free | 0.28700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4m4y |
RMSD bond length | 0.002 |
RMSD bond angle | 0.441 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.770 | 3.310 |
High resolution limit [Å] | 3.250 | 3.250 |
Rpim | 0.053 | |
Number of reflections | 24917 | 1320 |
<I/σ(I)> | 12 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.6 | |
CC(1/2) | 1.000 | 0.670 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M sodium acetate, pH 6.2, 20% PEG3350 |