Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-02-23 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.97932 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 175.134, 176.934, 509.703 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.730 - 3.100 |
| R-factor | 0.1943 |
| Rwork | 0.194 |
| R-free | 0.24700 |
| Structure solution method | SAD |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.525 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.800 | 3.210 |
| High resolution limit [Å] | 3.100 | 3.100 |
| Rmerge | 0.090 | 0.149 |
| Number of reflections | 271071 | 19970 |
| <I/σ(I)> | 30.9 | |
| Completeness [%] | 94.7 | |
| Redundancy | 3.3 | |
| CC(1/2) | 0.950 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIQUID DIFFUSION | 277 | 0.1M HEPES, pH 7.5, 0.2M NaCl and 16-20% PEG-3000 |
