8TTD
Structure of VPS29 complexed with Fam21A repeat 21 (1328-1341)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-21 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.95365 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 43.342, 43.342, 165.139 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 36.602 - 2.011 |
R-factor | 0.1873 |
Rwork | 0.184 |
R-free | 0.24110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.053 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.280 | 2.060 |
High resolution limit [Å] | 2.010 | 2.010 |
Rmerge | 0.052 | 0.475 |
Rmeas | 0.053 | 0.488 |
Rpim | 0.013 | 0.110 |
Total number of observations | 239643 | 17499 |
Number of reflections | 12765 | 911 |
<I/σ(I)> | 25.4 | 4.5 |
Completeness [%] | 99.9 | |
Redundancy | 18.8 | 19.2 |
CC(1/2) | 1.000 | 0.972 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M Magnesium Formate, 20% PEG3350 |