8T7L
Copper bound HftA from Treponema denticola
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-08-04 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.95374 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.510, 78.160, 150.270 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.170 - 1.890 |
R-factor | 0.2091 |
Rwork | 0.208 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pjl |
RMSD bond length | 0.007 |
RMSD bond angle | 0.912 |
Data reduction software | autoPROC |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.170 | 1.990 |
High resolution limit [Å] | 1.890 | 1.890 |
Rmerge | 0.139 | 0.080 |
Number of reflections | 30767 | 1100 |
<I/σ(I)> | 11.9 | |
Completeness [%] | 99.9 | 99.2 |
Redundancy | 12.6 | 11.3 |
CC(1/2) | 0.997 | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 291 | Sodium citrate, Ammonium sulphate, glycerol |