8SJN

[3T13] Self-assembling left-handed tensegrity triangle with 13 interjunction base pairs and R3 symmetry

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-07-18
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.00744
Spacegroup name	H 3
Unit cell lengths	163.006, 163.006, 106.056
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	37.610 - 7.300
R-factor	0.1457
Rwork	0.143
R-free	0.21660
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	8d93
RMSD bond length	0.004
RMSD bond angle	0.684
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	84.793	84.793	8.465
High resolution limit [Å]	7.299	14.575	7.299
Number of reflections	1102	184	183
<I/σ(I)>	4.7	10.2	0.8
Completeness [%]	82.1	99.5
Redundancy	9.5	9.1	9.9
CC(1/2)	0.995	0.994	0.305

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.8	293	100 mM MOPS, 1.25 M magnesium sulfate