8S4S
PrgE from plasmid pCF10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-11-13 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.9677 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.175, 58.170, 87.099 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.377 - 2.700 |
Rwork | 0.234 |
R-free | 0.27770 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.670 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX (1.20.1-4487) |
Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.380 | 2.560 |
High resolution limit [Å] | 2.515 | 2.515 |
Rmeas | 0.139 | 1.718 |
Number of reflections | 10486 | 537 |
<I/σ(I)> | 21.4 | 2.39 |
Completeness [%] | 99.6 | 100 |
Redundancy | 33.1 | 35.04 |
CC(1/2) | 0.999 | 0.852 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M LiSO4, 0.1 M K Phos Cit pH 4.2, 20 %w/v PEG 1K |