8S45
CdaA-E05 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-08-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9677 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.750, 64.710, 129.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.720 - 1.690 |
R-factor | 0.1983 |
Rwork | 0.196 |
R-free | 0.23570 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 39.720 | 50.000 | 1.790 |
High resolution limit [Å] | 1.690 | 17.000 | 1.690 |
Rmerge | 0.050 | 0.017 | 2.055 |
Rmeas | 0.057 | 0.020 | 2.350 |
Number of reflections | 74891 | 66 | 11891 |
<I/σ(I)> | 13.12 | ||
Completeness [%] | 99.0 | ||
Redundancy | 4.4 | ||
CC(1/2) | 0.999 | 1.000 | 0.521 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 3.7 M NaCl, 0.1M Na-HEPES pH 8.5 and 3 % DMSO |