Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-09-05 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.00002 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 86.911, 86.921, 103.297 |
| Unit cell angles | 90.00, 94.38, 90.00 |
Refinement procedure
| Resolution | 45.830 - 2.590 |
| R-factor | 0.2413 |
| Rwork | 0.239 |
| R-free | 0.28750 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.821 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.830 | 2.680 |
| High resolution limit [Å] | 2.590 | 2.590 |
| Rmerge | 0.082 | 0.556 |
| Number of reflections | 47823 | 4734 |
| <I/σ(I)> | 8.25 | |
| Completeness [%] | 99.5 | |
| Redundancy | 3.3 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 293 | 16% PEG8000 0.04M potassium phosphate dibasic 20% glycerol |
