Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-08-07 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.738, 214.335, 55.766 |
| Unit cell angles | 90.00, 97.09, 90.00 |
Refinement procedure
| Resolution | 55.340 - 1.872 |
| R-factor | 0.1952 |
| Rwork | 0.193 |
| R-free | 0.23590 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.100 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | CSearch |
| Refinement software | BUSTER |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.340 | 1.890 |
| High resolution limit [Å] | 1.870 | 1.870 |
| Rmeas | 0.039 | 0.620 |
| Number of reflections | 87176 | 2102 |
| <I/σ(I)> | 10.9 | 1.7 |
| Completeness [%] | 99.0 | 93 |
| Redundancy | 3.2 | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.5M K formate 15% PEG 3350 0.1M pH=8 Bis-Tris propane/HCl |
