Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-04-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.96862 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.902, 212.545, 55.811 |
| Unit cell angles | 90.00, 96.79, 90.00 |
Refinement procedure
| Resolution | 45.580 - 1.929 |
| R-factor | 0.195 |
| Rwork | 0.193 |
| R-free | 0.22360 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.100 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | CSearch |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.580 | 1.970 |
| High resolution limit [Å] | 1.929 | 1.929 |
| Rmeas | 0.047 | 0.726 |
| Number of reflections | 77010 | 4165 |
| <I/σ(I)> | 11.8 | 2 |
| Completeness [%] | 96.6 | 89.4 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.5M K formate 15% PEG 3350 0.1M pH=8 Bis-Tris propane/HCl |
